The lack of more sophisticated technical equipment and expertise prevented further analysis until Mr Valcárcel visited the unique on-site facilities in the UCL Institute of Archaeology last year, where scanning electron microscopy and X-ray microanalytical techniques were applied to the artefacts.
"The key to deciphering where metals come from is to look at their geochemical signature," explains Dr Martinón-Torres. "The technology to exploit copper and silver was unknown to the Taíno but was in common use on mainland South American, which strongly suggests that the alloy was imported from within America. However, brass production was unknown outside Europe.
"Brass is an alloy composed of copper and zinc but, depending on where the constitute metals come from, they also have traces of other elements. Using techniques equivalent to looking at the DNA of the metal we were able to show that minute iron, lead and tin impurities were consistent with brass objects from Nuremberg at this time.
"Although we lack detailed information on the supply of brass in 16th century Spain, it seems very plausible that the German metal used for these tubes could have reached Spain via established commercial routes before being brought to Cuba."
Professor Thilo Rehren, of the UCL Institute of Archaeology, and senior author of the study, says: "Acquiring gold of the New World quickly became one of the major aspirations of the European colonists, and ethnohistorical accounts highlight how they endeavoured to liaise with the emerging local elites to barter for their circulating gold and exploit some of their other natural resources. The relationship between Europeans and Americans, in which metals seem to have played a very significant role, dramatically affected the later history of both peoples. The removal of noble metals had a significant impact on the later economy and goes some way to explaining why Europe is rich today compared with Cuba."
Roy Stephenson, the Museum of London's archaeological archive manager, added: "This is fascinating work carried out by UCL which will shed light on what appears to be quite dreary and repetitive finds, but in reality tells a compelling story about international trade."
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Adapted from materials provided by University College London, via EurekAlert!, a service of AAAS.
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